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化工专业英语翻译2determined with a Redlich-Kwong-Soave equation of s

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化工专业英语翻译2
determined with a Redlich-Kwong-Soave equation of state

with Boston-Mathias modification, through the Aspen Proper-

ties code. The pressure inside the reactor is controlled and

regulated with a back pressure controller (BPC; Brooks 5866

series). A rupture disk is located before the BPC for safety

reasons. A bypass is used to achieve the desired pressure inside

the reactor more rapidly. The liquid phase is fed in through a

syringe pump (Teledyne ISCO model 500D), connected to a

pressure transducer and computer controlled. The syringe

temperature can be controlled. Gas and liquids mix at a

T-connection before the reactor. A regulation valve is used to

sample the instantaneous liquid phase, while a 1.5 L tank

provides gas-liquid separation, accumulating all the liquid

product. All the piping is made of stainless steel AISI 316, 1/8

in. size. The catalyst bed (0.5 cm long) is placed between two

quartz wool plugs. Above the upstream quartz wool plug, quartz

sand is used to improve mixing. Temperature inside the reactor

is measured with a K-thermocouple before the catalyst bed. The

apparatus is in a fume hood, with a H2 sensor that can

automatically switch off H2 flow to the reactor.

H2O2 Experiments and Analyses. H2O2 decomposition and

hydrogenation were investigated first, at 10 bar and -10 °C,

with 0.5% H2O2 in methanol as the liquid phase, varying its

flow rate (0.5, 1, and 2 mL/min). The gas mixture was either

N2/CO2 (20/80% mol) for pure decomposition, or H2/N2/CO2

(2/18/80% mol) for hydrogenation experiments (N2 replaces O2),

varying its flow rates (0.1, 1, 2, 2.7, 4, 6, 9,and 12 mL/min)
与Redlich-Kwong-Soave状态方程确定
波士顿马蒂亚斯Modifi阳离子,通过适当的白杨—
关系代码.反应器内的压力控制
一个背压控制器调节(BPC;布鲁克斯5866
系列).破裂盘位于前安全BPC
原因.旁路是用来实现所需的内部压力
反应更迅速.液相是美联储通过
注射泵(Teledyne公司新型500D),连接到一个
压力传感器和计算机控制.注射器
温度可以控制.气体和液体混合在一个
在反应器的T接.调节阀用于
样品的瞬时液相,而1.5 L罐
提供气液分离,积累的所有液体
产品.所有的管道是由不锈钢AISI 316,1 / 8
在.大小.催化剂床(0.5厘米长)之间放置两个
石英棉塞.在上游的石英棉塞,石英
沙子是用来改善混合.反应器内的温度
是在催化剂床层的K型热电偶测量.的
装置在油烟机,一个可以H2传感器
自动切断氢气fl如何反应.
过氧化氢的实验和分析.过氧化氢分解
研究了fiRST进行加氢,在10条和10°C,
用0.5%过氧化氢在甲醇作为液相,改变其
fl流量(0.5,1,和2毫升/分钟).气体混合物是
氮气/二氧化碳(20/80%μmol)纯分解,或H2/N2和CO
(2 / 18 / 80% mol)加氢实验(N2取代O2),
不同的flOW率(0.1,1,2,2.7,4,6,9,和12毫升/分钟)