英语翻译Synthesis of [C2NH8]2[Co3(HPO3)4] 3In a typical synthesi

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英语翻译
Synthesis of [C2NH8]2[Co3(HPO3)4] 3
In a typical synthesis,a reaction mixture of Co(CH3-
COO)2$4H2O (3 mmol),CoCl2$ 6H2O (0.75 mmol),piperazine
(5 mmol),H3PO3 (0.9 mL,50% in water) and DMF (20 ml) was
sealed in an Teflon-lined steel autoclave and heated at 120 \3C for
2 d.The resulting blue block crystals were isolated by filtration,
washed with ethanol and dried in air.The agreement between the
experimental and simulated XRD patterns indicated the phase
purity of the product (Fig.S1c†).Analysis found
(%)[C2NH8]2[Co3(HPO3)4]:Co,30.32; P,21.17; C,8.07; H,3.52;
N,4.63.Calc.(%):Co,30.06; P,21.06; C,8.15; H,3.40; N,4.75.
The UV-vis diffuse-reflectance spectrum of 3 exhibits three
absorption maxima at 544,583,and 624 nm (Fig.S2†).The TG
curve of 3 shows a weight loss of 14.28% in the temperature range
of 160–400 \3C,corresponding to the loss of the dimethylamine
molecules (calc.15.62%) (Fig.S3c†).

合成[C2NH8]2[二氧化碳(HPO3)4)3在一个典型的合成,反应混合物的Co(CH3-COO)2 4美元的水(3中和),CoCl2 6美元h2o(0.75中和)、哌嗪(5中和),H3PO3(0.9毫升,50%水)和DMF(20毫升)wassealed在聚四氟乙烯内衬钢高压蒸汽和加热在120 C于d.由此产生的蓝色块晶体分离过滤,水洗与乙醇和干空气.theexperimental之间的协议和模拟x射线衍射模式表明了产品的phasepurity(无花果.S1c†).分析发现(%)(C2NH8]2[二氧化碳(HPO3)4]:有限公司,21.17;30.32;P C,H,3.52;8.07;4.63 N,.Calc.(%):有限公司,21.06;30.06;P C,H,3.40;8.15;4.75 N,.紫外可见漫反射光谱的threeabsorption 3展品最大值在544、583和624海里(无花果.S2†).这个TGcurve 3显示了一个减肥的14.28% rangeof温度160 - 400度,相应的损失,dimethylaminemolecules(calc.15.62%)(无花果.S3c†).

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